{"id":459794,"date":"2024-10-20T10:06:01","date_gmt":"2024-10-20T10:06:01","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-iso-ts-9516-22024\/"},"modified":"2024-10-26T18:39:22","modified_gmt":"2024-10-26T18:39:22","slug":"bsi-pd-iso-ts-9516-22024","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-iso-ts-9516-22024\/","title":{"rendered":"BSI PD ISO\/TS 9516-2:2024"},"content":{"rendered":"
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 4 Principle 5 Reagents and materials <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 6 Apparatus <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 7 Sampling and samples 7.1 Laboratory sample 7.2 Preparation of test samples 7.2.1 General 7.2.2 Method specified in ISO 2596 <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 7.2.3 Method specified in ISO 7764 8 Procedure 8.1 General <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 8.2 Number of determinations 8.3 Check analysis and blank test 8.4 Preparation of discs 8.4.1 Weighing <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 8.4.2 Mixing 8.4.3 Fusion 8.4.4 Casting 8.4.5 Visual inspection 8.4.6 Disc storage <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 8.4.7 Cleaning of platinum ware 8.4.8 Test discs 8.5 Measurement 8.5.1 General <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | 8.5.2 Effect of errors or omissions <\/td>\n<\/tr>\n | ||||||
19<\/td>\n | 8.5.3 Analytical lines 8.5.4 XRF generator settings <\/td>\n<\/tr>\n | ||||||
22<\/td>\n | 8.5.5 Crystals 8.5.6 Line overlaps 8.5.7 Collimators 8.5.8 Pulse height settings 8.5.9 Counting time <\/td>\n<\/tr>\n | ||||||
23<\/td>\n | 8.5.10 Simultaneous instruments 8.5.11 Sample holders <\/td>\n<\/tr>\n | ||||||
24<\/td>\n | 8.5.12 Measurement sequence 8.6 Drift correction 8.6.1 Preparation of drift correction monitor discs <\/td>\n<\/tr>\n | ||||||
25<\/td>\n | 8.6.2 Drift correction using monitor disc <\/td>\n<\/tr>\n | ||||||
27<\/td>\n | 9 Calculation of results 9.1 General <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | 9.2 Calibration equation <\/td>\n<\/tr>\n | ||||||
31<\/td>\n | 9.3 Calculation of alpha coefficient <\/td>\n<\/tr>\n | ||||||
32<\/td>\n | 9.4 Correction for sample, flux and oxidizer mass 9.4.1 General 9.4.2 Correction of flux\/sample mass ratio 9.4.3 Correction of remaining oxidizer\/sample mass ratio <\/td>\n<\/tr>\n | ||||||
33<\/td>\n | 9.4.4 Mass ratio correction constant in calibration Equation 1 9.5 Calculation of calibration 9.5.1 Preparation of calibration discs <\/td>\n<\/tr>\n | ||||||
36<\/td>\n | 9.5.2 Calculation of concentrations of calibration discs <\/td>\n<\/tr>\n | ||||||
37<\/td>\n | 9.5.3 Measurement of calibration discs 9.5.4 Calculation of calibration coefficients <\/td>\n<\/tr>\n | ||||||
41<\/td>\n | 9.6 Calculation of concentrations 9.6.1 Calculation of flux\/sample and remaining oxidizer\/sample mass ratios <\/td>\n<\/tr>\n | ||||||
42<\/td>\n | 9.6.2 Calculation of initial concentration 9.6.3 Calculation of concentrations <\/td>\n<\/tr>\n | ||||||
43<\/td>\n | 9.6.4 Conversion from oxide to element concentrations 10 General treatment of results 10.1 Background equivalent concentration (BEC) <\/td>\n<\/tr>\n | ||||||
44<\/td>\n | 10.2 Determination of analytical result 10.3 Check for trueness <\/td>\n<\/tr>\n | ||||||
45<\/td>\n | 10.4 Calculation of the final result <\/td>\n<\/tr>\n | ||||||
46<\/td>\n | 10.5 Oxide factors 11 Test report <\/td>\n<\/tr>\n | ||||||
47<\/td>\n | Annex A (normative) Preparation of Flux A and Flux D <\/td>\n<\/tr>\n | ||||||
49<\/td>\n | Annex B (normative) Preparation of Flux B and Flux C <\/td>\n<\/tr>\n | ||||||
50<\/td>\n | Annex C (normative) Standard deviation of specimen preparation <\/td>\n<\/tr>\n | ||||||
52<\/td>\n | Annex D (normative) Spectrometer precision tests <\/td>\n<\/tr>\n | ||||||
56<\/td>\n | Annex E (informative) Theoretical derivation of correction term in calibration <\/td>\n<\/tr>\n | ||||||
61<\/td>\n | Annex F (informative) Calculation of correction coefficients using the FP method (fundamental parameter method) <\/td>\n<\/tr>\n | ||||||
64<\/td>\n | Annex G (informative) Calculation of calibration coefficients and correction alphas by the least square method <\/td>\n<\/tr>\n | ||||||
68<\/td>\n | Annex H (informative) Calculation of counting time <\/td>\n<\/tr>\n | ||||||
71<\/td>\n | Annex I (informative) Air cooling block for fused discs <\/td>\n<\/tr>\n | ||||||
72<\/td>\n | Annex J (normative) Flowchart for acceptance of results <\/td>\n<\/tr>\n | ||||||
73<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Iron ores. Determination of various elements by X-ray fluorescence spectrometry – Single element calibration procedure<\/b><\/p>\n |