{"id":420980,"date":"2024-10-20T06:33:49","date_gmt":"2024-10-20T06:33:49","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-171942019\/"},"modified":"2024-10-26T12:17:09","modified_gmt":"2024-10-26T12:17:09","slug":"bs-en-171942019","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-171942019\/","title":{"rendered":"BS EN 17194:2019"},"content":{"rendered":"
This document’s method of analysis is applicable for the determination of:<\/p>\n
deoxynivalenol (DON) in the tested range of 100 \u03bcg\/kg to 3 300 \u03bcg\/kg,<\/p>\n<\/li>\n
aflatoxin B1 (AfB1) in the tested range of 2,5 \u03bcg\/kg to 440 \u03bcg\/kg,<\/p>\n<\/li>\n
fumonisin B1 (FB1) in the tested range of 690 \u03bcg\/kg to 7 500 \u03bcg\/kg,<\/p>\n<\/li>\n
fumonisin B2 (FB2) in the tested range of 200 \u03bcg\/kg to 2 500 \u03bcg\/kg,<\/p>\n<\/li>\n
T-2 toxin in the tested range of 7,5 \u03bcg\/kg to 360 \u03bcg\/kg,<\/p>\n<\/li>\n
HT-2 toxin in the tested range of 14 \u03bcg\/kg to 1 800 \u03bcg\/kg,<\/p>\n<\/li>\n
zearalenone (ZEN) in the tested range of 30 \u03bcg\/kg to 600 \u03bcg\/kg, and<\/p>\n<\/li>\n
ochratoxin A (OTA) in the tested range of 10 \u03bcg\/kg to 230 \u03bcg\/kg<\/p>\n<\/li>\n<\/ul>\n
in cereals and cereal-based compound feed by liquid-chromatography tandem mass spectrometry (LCMS\/ MS). The actual working ranges could extend beyond the tested ranges.<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | 5 Reagents <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 6 Apparatus <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 7 Procedure 7.1 Sample preparation <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 7.2 Extraction 7.2.1 Introduction 7.2.2 Dry samples 7.2.3 Slurry 7.3 Test solution <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 7.4 Spiking procedure 8 Measurements 8.1 General 8.2 LC conditions 8.3 MS conditions <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 8.4 Batch composition 8.5 Peak identification 8.6 Determination of mycotoxins in calibration and test solutions 8.7 Calibration <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 9 Determination of mass fraction <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 10 Precision 10.1 Interlaboratory study 10.2 Repeatability <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 10.3 Reproducibility 11 Test report <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | Annex A (informative)Precision data <\/td>\n<\/tr>\n | ||||||
27<\/td>\n | Annex B (informative)Examples B.1 General B.2 Example 1 B.2.1 General B.2.2 LC conditions <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | B.2.3 MS conditions <\/td>\n<\/tr>\n | ||||||
29<\/td>\n | B.3 Example 2 B.3.1 General B.3.2 LC conditions <\/td>\n<\/tr>\n | ||||||
30<\/td>\n | B.3.3 MS conditions <\/td>\n<\/tr>\n | ||||||
32<\/td>\n | Annex C (informative)Example chromatograms <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Animal feeding stuffs: Methods of sampling and analysis. Determination of Deoxynivalenol, Aflatoxin B1, Fumonisin B1 & B2, T-2 & HT-2 toxins, Zearalenone and Ochratoxin A in feed materials and compound feed by LC-MS\/MS<\/b><\/p>\n |