{"id":315280,"date":"2024-10-19T21:43:36","date_gmt":"2024-10-19T21:43:36","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-157212013\/"},"modified":"2024-10-25T19:51:49","modified_gmt":"2024-10-25T19:51:49","slug":"bs-en-157212013","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-157212013\/","title":{"rendered":"BS EN 15721:2013"},"content":{"rendered":"
This European Standard specifies a gas chromatographic method for ethanol, in which higher alcohols (propan-1-ol, butan-1-ol, butan-2-ol, 2-methylpropan-1-ol (isobutanol), 2-methylbutan-1-ol, and 3-methylbutan-1-ol) from 0,1 % up to 2,5 % (m\/m<\/i>), methanol from 0,1 % up to 3 % (m\/m<\/i>) and other impurities, in the range from 0,1 % up to 2 % (m\/m<\/i>) are determined.<\/p>\n
Impurities are all the compounds not attributed to the groups of higher alcohols or methanol.<\/p>\n
\nNOTE 1 The European ethanol blending component specification[1]<\/sup> sets a limit for the combined result of ethanol + higher alcohols, not the ethanol content itself.<\/p>\n<\/blockquote>\n
Due to possible interferences, the method is not applicable to denatured ethanol samples.<\/p>\n
Water, if present in the sample, is not included in this analysis, because a signal for water is not visible in the chromatogram. Therefore, if “alcohol content” is called up in a specification, water needs to be considered separately in the calculations.<\/p>\n
\nNOTE 2 For the purposes of this European Standard, the term \u201c% (m\/m<\/i>)\u201d is used to represent the mass fraction (\u03c9<\/i>).<\/p>\n<\/blockquote>\n
PDF Catalog<\/h4>\n
\n
\n PDF Pages<\/th>\n PDF Title<\/th>\n<\/tr>\n \n 7<\/td>\n 1 Scope
2 Normative references
3 Principle
4 Reagents and materials <\/td>\n<\/tr>\n\n 8<\/td>\n 5 Apparatus <\/td>\n<\/tr>\n \n 9<\/td>\n 6 Sampling <\/td>\n<\/tr>\n \n 10<\/td>\n 7 Procedure
7.1 General
7.2 General considerations for preparation and handling of solutions
7.3 Preparation of solutions for Procedure A
7.3.1 Calibration stock solution (E) for Procedure A <\/td>\n<\/tr>\n\n 11<\/td>\n 7.3.2 Internal standard stock solution (ES) for Procedure A
7.3.3 Calibration solution (FS1) for Procedure A
7.3.4 Preparation of sample (S) for Procedure A
7.4 Preparation of solutions for Procedure B
7.4.1 Calibration stock solution (E) for Procedure B <\/td>\n<\/tr>\n\n 12<\/td>\n 7.4.2 Internal standard stock solution (ES) for Procedure B
7.4.3 Calibration solution (FS1) for Procedure B
7.4.4 Preparation of sample (S) for Procedure B
7.5 Determination
7.5.1 Gas chromatograph analysis conditions <\/td>\n<\/tr>\n\n 13<\/td>\n 7.5.2 Determination of response factors <\/td>\n<\/tr>\n \n 14<\/td>\n 7.5.3 Recording the chromatogram
7.5.4 Performance checks
8 Calculation
8.1 Content of individual compounds
8.2 Calculation of group contents <\/td>\n<\/tr>\n\n 15<\/td>\n 8.3 Expression of results
9 Precision
9.1 General
9.2 Repeatability
9.3 Reproducibility <\/td>\n<\/tr>\n\n 16<\/td>\n 10 Test report <\/td>\n<\/tr>\n \n 17<\/td>\n Annex A (informative) Examples of chromatograms <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Ethanol as a blending component for petrol. Determination of higher alcohols, methanol and other impurities. Gas chromatographic method<\/b><\/p>\n
\n\n
\n Published By<\/td>\n Publication Date<\/td>\n Number of Pages<\/td>\n<\/tr>\n \n BSI<\/b><\/a><\/td>\n 2013<\/td>\n 26<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":315284,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1074,2641],"product_tag":[],"class_list":{"0":"post-315280","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-75-160-20","7":"product_cat-bsi","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/315280","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/315284"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=315280"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=315280"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=315280"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}