{"id":290928,"date":"2024-10-19T19:44:54","date_gmt":"2024-10-19T19:44:54","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-cen-ts-164902013\/"},"modified":"2024-10-25T16:45:50","modified_gmt":"2024-10-25T16:45:50","slug":"bsi-pd-cen-ts-164902013","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-cen-ts-164902013\/","title":{"rendered":"BSI PD CEN\/TS 16490:2013"},"content":{"rendered":"
In Regulation (EC) No. 2003\/2003 [2] tolerance limits are mentioned for nutrient contents in mineral fertilizers (Annex II of Regulation (EC) No. 2003\/2003) as well as prescribed methods for control purposes (Annex IV of Regulation (EC) No. 2003\/2003).<\/p>\n
Prior to the work done by CEN\/TC 260 following Mandate M\/335, no statistical data were available for the official analytical methods to be applied. Due to the standardization work done for this mandate, statistical data have been generated as ring testing was a major topic in this mandate.<\/p>\n
This Technical Specification describes to what extent the presently applied tolerances are in line with the obtained precision data from the analytical methods studied.<\/p>\n
The purpose of this document is to give feedback on the applied tolerances within Regulation (EC) No. 2003\/2003 based on the method evaluation done as an outcome of the work executed by CEN\/TC 260\/WG 7 according to Mandate M\/335. This evaluation of the tolerances was part of Mandate M\/418.<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
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7<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | 4 Statistical method validation 4.1 General 4.2 Approach taken by CEN\/TC 260\/WG 7 4.2.1 Product selection 4.2.2 Samples and their preparation 4.2.3 Laboratories involved 4.2.4 Data evaluation 4.3 Statistical data: results versus tolerances <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 4.4 Refined statistical analysis 4.5 Field data <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 5 Conclusions <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | Annex A (informative) Statistical data of the inter-laboratory tests and findings A.1 General A.2 Nitrogen <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | A.3 Phosphate <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | A.4 Potassium A.5 Sulfur <\/td>\n<\/tr>\n | ||||||
20<\/td>\n | A.6 Chloride A.7 Secondary nutrients A.7.1 Manganimetric determination of extracted calcium following precipitation in the form of oxalate (EC method 8.6, EN 16196) <\/td>\n<\/tr>\n | ||||||
22<\/td>\n | A.7.2 Determination of magnesium by atomic absorption spectrometry (EC method 8.7, EN 16197) <\/td>\n<\/tr>\n | ||||||
24<\/td>\n | A.7.3 Determination of magnesium by complexometry (EC method 8.8, EN 16198) <\/td>\n<\/tr>\n | ||||||
25<\/td>\n | A.7.4 Determination of extracted sodium flame-emission spectrometry (EC method 8.10, EN 16199) <\/td>\n<\/tr>\n | ||||||
28<\/td>\n | Annex B (informative) Refined statistical evaluation B.1 General B.2 Meaning of symbols <\/td>\n<\/tr>\n | ||||||
29<\/td>\n | B.3 Tolerances for SO3 <\/td>\n<\/tr>\n | ||||||
30<\/td>\n | B.4 Tolerances for CaO, MgO. Na2O and Cl <\/td>\n<\/tr>\n | ||||||
34<\/td>\n | B.5 Refinement of results B.6 Comments <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Fertilizers. Comparison of the CEN\/TC 260\/WG 7 ring test results with tolerances given in the Regulation (EC) Nr 2003\/2003 Annex II and conclusions<\/b><\/p>\n |