{"id":159038,"date":"2024-10-19T09:32:10","date_gmt":"2024-10-19T09:32:10","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-e2866-2016\/"},"modified":"2024-10-25T01:50:18","modified_gmt":"2024-10-25T01:50:18","slug":"astm-e2866-2016","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-e2866-2016\/","title":{"rendered":"ASTM-E2866 2016"},"content":{"rendered":"

ASTM E2866-12-Reapproved2016<\/h3>\n

Historical Standard: Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography\/Tandem Mass Spectrometry<\/h4>\n
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ASTM E2866<\/h4>\n

Scope<\/strong><\/p>\n

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1.1<\/span> This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography\/tandem mass spectrometry (LC\/MS\/MS). OPs are qualitatively and quantitatively determined by this method.<\/p>\n<\/p><\/div>\n

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1.2<\/span> Units\u2014<\/span>The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.<\/p>\n<\/p><\/div>\n

\n

1.3<\/span> The Method Detection Limit2<\/span><\/span> (MDL), electrospray ionization (ESI) mode and Reporting Range3<\/span><\/span> for the OPs are listed in Table 1<\/span>.<\/p>\n

<\/div>\n<\/p><\/div>\n
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1.4<\/span> This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.<\/i><\/p>\n<\/p><\/div>\n

Keywords<\/strong><\/p>\n

liquid chromatography; mass spectrometry; organophosphonates; pressurized fluid extraction; soil;<\/p>\n

ICS Code<\/strong><\/p>\n

ICS Number Code 13.080.10 (Chemical characteristics of soil)<\/p>\n

DOI:<\/strong> 10.1520\/E2866-12R16<\/p>\n<\/div>\n","protected":false},"excerpt":{"rendered":"

E2866-12(2016) Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid Chromatography\/Tandem Mass Spectrometry<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
ASTM<\/b><\/a><\/td>\n2016<\/td>\n15<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":159042,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[223,2637],"product_tag":[],"class_list":{"0":"post-159038","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-13-080-10","7":"product_cat-astm","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/159038","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/159042"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=159038"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=159038"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=159038"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}