BS ISO 20903:2019 – TC:2020 Edition
$186.33
Tracked Changes. Surface chemical analysis. Auger electron spectroscopy and X-ray photoelectron spectroscopy. Methods used to determine peak intensities and information required when reporting results
| Published By | Publication Date | Number of Pages |
| BSI | 2020 | 52 |
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 1 | compares BS ISO 20903:2019 |
| 2 | TRACKED CHANGES Text example 1 — indicates added text (in green) |
| 3 | National foreword Compliance with a British Standard cannot confer immunity from legal obligations. Amendments/corrigenda issued since publication |
| 4 | Surface chemical analysis — Auger electron spectroscopy and X-ray photoelectron spectroscopy — Methods used to determine peak intensities and information required when reporting results |
| 5 | COPYRIGHT PROTECTED DOCUMENT |
| 7 | Foreword |
| 8 | Introduction |
| 9 | Surface chemical analysis — Auger electron spectroscopy and X-ray photoelectron spectroscopy — Methods used to determine peak intensities and information required when reporting results 1 Scope 2 Normative references 3 Terms and definitions 4 Symbols and abbreviated terms |
| 10 | 5 Methods for peak-intensity determination — direct spectrum 5.1 General Figure 1 — Illustration of procedure involved in the determination of the intensity of a single peak in an X-ray photoelectron spectrum (as described in 5.2 and 5.3). |
| 11 | 5.2 Selection and subtraction of an inelastic background |
| 12 | 5.3 Measurement of peak intensity 5.3.1 Measurement of peak height 5.3.2 Measurement of peak area |
| 13 | 5.4 Measurement of a peak intensity with computer software 5.5 Measurement of peak intensities for a spectrum with overlapping peaks |
| 14 | Figure 2 — X-ray photoelectron spectrum measured with unmonochromated Al Kα X-rays for 5.6 Uncertainty in measurement of peak area |
| 15 | 6 Methods for peak intensity determination — Auger-electron differential spectrum 6.1 General |
| 16 | 6.2 Measurement of Auger-electron differential intensity Figure 3 — Schematic diagram of an Auger-electron differential spectrum indicating measurements of peak-to-peak and peak-to-background intensities 6.3 Uncertainties in measurement of Auger-electron differential intensity |
| 18 | a) Secondary electron micrograph (SEM) and direct and differentiated Auger C KLL spectra of a diamond particle and the graphite background Figure 4 — Secondary electron micrograph (SEM), Auger spectra and Auger maps from a diamond particle on a graphite substrate |
| 19 | a) Auger spectra of Zn oxide and Zn metal used as basis spectra for LLS separation of the two Zn species in the depth profile shown in Figure 5 c) Figure 5 — Auger spectra of zinc, acquired during a depth profile through a layer of zinc oxide 7 Reporting of methods used to measure peak intensities 7.1 General requirements |
| 20 | 7.2 Methods used to determine peak intensities in direct spectra 7.2.1 Intensity measurement for a single peak, as described in 5.2 and 5.3 7.2.2 Intensity measurements from peak fitting, as described in 5.4 and 5.5 7.3 Methods used to obtain and determine peak intensities in Auger-electron differential spectra 7.3.1 Method used to obtain differential spectra 7.3.2 Method used to determine peak intensities, as described in 6.2 |
| 22 | Annex B |
| 24 | Bibliography |
| 28 | undefined |
| 32 | Foreword |
| 33 | Introduction |
| 35 | 1 Scope 2 Normative references 3 Terms and definitions 4 Symbols and abbreviated terms |
| 36 | 5 Methods for peak-intensity determination — direct spectrum 5.1 General |
| 37 | 5.2 Selection and subtraction of an inelastic background |
| 38 | 5.3 Measurement of peak intensity 5.3.1 Measurement of peak height 5.3.2 Measurement of peak area |
| 39 | 5.4 Measurement of a peak intensity with computer software 5.5 Measurement of peak intensities for a spectrum with overlapping peaks |
| 40 | 5.6 Uncertainty in measurement of peak area |
| 41 | 6 Methods for peak intensity determination — Auger-electron differential spectrum 6.1 General 6.2 Measurement of Auger-electron differential intensity |
| 42 | 6.3 Uncertainties in measurement of Auger-electron differential intensity |
| 44 | 7 Reporting of methods used to measure peak intensities 7.1 General requirements 7.2 Methods used to determine peak intensities in direct spectra 7.2.1 Intensity measurement for a single peak, as described in 5.2 and 5.3 |
| 45 | 7.2.2 Intensity measurements from peak fitting, as described in 5.4 and 5.5 7.3 Methods used to obtain and determine peak intensities in Auger-electron differential spectra 7.3.1 Method used to obtain differential spectra 7.3.2 Method used to determine peak intensities, as described in 6.2 |
| 46 | Annex A (informative) Instrumental effects on measured intensities |
| 47 | Annex B (informative) Useful integration limits for determination of peak intensities in XPS spectra |
| 49 | Bibliography |
