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BS ISO 11236:2017

$142.49

Rubber compounding ingredients. p-Phenylenediamine antidegradants (PPDs). Test methods

Published By Publication Date Number of Pages
BSI 2017 30
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This document applies to a variety of substituted p-phenylenediamine antidegradants (PPDs) used in the rubber industry. The three general classes of PPDs are dialkyl, alkyl-aryl and diaryl, which are used to impart ozone resistance to rubber.

The following test methods are of greatest significance in assessing the purity of production PPDs, and hence their suitability for use in rubber. They are specified in this document as follows:

  • determination of purity by gas chromatography (GC);

  • determination of purity by high-performance liquid chromatography (HPLC);

  • determination of ash;

  • determination of volatile matter.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
8 4 Abbreviated terms
5 Use and classification
9 6 Sampling and repeat determinations
7 Determination of purity by gas chromatography (GC)
7.1 General
7.2 Interference
7.3 Apparatus
11 7.4 Calibration and standardization
7.5 Procedure
7.5.1 Sample preparation
7.5.2 Procedure A
17 7.6 Calculation
7.7 Precision and bias
7.8 Test report
8 Determination of purity by high-performance liquid chromatography (HPLC)
8.1 General
8.2 Apparatus
18 8.3 Reagents
8.4 Procedure
20 8.5 Calculation
8.6 Precision and bias
21 8.7 Test report
9 Determination of ash
9.1 General
9.2 Apparatus
9.3 Procedure
22 9.4 Calculation
9.5 Precision and bias
9.6 Test report
10 Determination of volatile matter
10.1 General
23 10.2 Apparatus
10.3 Preparation of sample
10.4 Procedure
10.5 Calculation
10.6 Precision and bias
24 10.7 Test report
25 Annex A (informative) Precision and bias
28 Bibliography
BS ISO 11236:2017
$142.49