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BS EN ISO 643:2020

$142.49

Steels. Micrographic determination of the apparent grain size

Published By Publication Date Number of Pages
BSI 2020 28
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This document specifies a micrographic method of determining apparent ferritic or austenitic grain size in steels. It describes the methods of revealing grain boundaries and of estimating the mean grain size of specimens with unimodal size distribution. Although grains are three-dimensional in shape, the metallographic sectioning plane can cut through a grain at any point from a grain corner, to the maximum diameter of the grain, thus producing a range of apparent grain sizes on the two-dimensional plane, even in a sample with a perfectly consistent grain size.

PDF Catalog

PDF Pages PDF Title
2 undefined
4 European foreword
Endorsement notice
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
3.1 Grains
8 3.2 General
4 Symbols
9 5 Principle
10 6 Selection and preparation of the specimen
6.1 Test location
11 6.2 Revealing ferritic grain boundaries
6.3 Revealing austenitic and prior-austenitic grain boundaries
6.3.1 General
6.3.2 “Bechet-Beaujard” method by etching with aqueous saturated picric acid solution
12 6.3.3 “Kohn” method by controlled oxidation
13 6.3.4 “McQuaid-Ehn” method by carburization at 925 °C
14 6.3.5 Proeutectoid ferrite method
15 6.3.6 Bainite or gradient-quench method
6.3.7 Sensitization of austenitic stainless and manganese steels
6.3.8 Other methods for revealing prior-austenitic grain boundaries
16 7 Characterization of grain size
7.1 Characterization by an index
7.1.1 Formulae
7.1.2 Assessment by comparison with standard grain size charts
17 7.1.3 Planimetric method
7.1.4 Estimation of the index
7.2 Characterization by the intercept method
7.2.1 Linear intercept segment method
18 7.2.2 Circular intercept segment method
19 7.2.3 Assessment of results
20 8 Test report
21 Annex A (informative) Summary of methods for revealing ferritic, austenitic or prior-austenitic grain boundaries in steels
22 Annex B (normative) Evaluation method
27 Bibliography
BS EN ISO 643:2020
$142.49