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BS EN ISO 22036:2024

BS EN ISO 22036:2024

$167.15

Environmental solid matrices. Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

Published By Publication Date Number of Pages
BSI 2024 40
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This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gallium (Ga), gadolinium (Gd), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu) magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tantalum (Ta), tellurium (Te), terbium (Tb), thallium (Tl), thulium (Tm), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), vanadium (V), yttrium (Y), ytterbium (Yb), zinc (Zn) and zirconium (Zr). The method is also applicable to other extracts or digests originating from, for example, DTPA extraction, fusion methods or total digestion methods, provided the user has verified the applicability. The method has been validated for the elements given in Table A.1 (sludge), Table A.2 (compost) and Table A.3 (soil). The method is applicable for other solid matrices and other elements as listed above, provided the user has verified the applicability. This method is also applicable for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products (EN 17200[22]). NOTE            Construction products include e.g. mineral-based products; bituminous products; metals; wood-based products; plastics and rubbers; sealants and adhesives; paints and coatings.

PDF Catalog

PDF Pages PDF Title
2 undefined
13 5.1 General
5.2 Spectral interferences
14 5.3 Non-spectral interferences
18 8.1 Cleaning of glassware
8.2 Instrument performance parameters
19 8.3 Instrument optimization
8.4 Instrument set-up
8.4.1 General requirements
8.4.2 Software method development, wavelength selection
8.4.3 Inter-element correction
8.4.4 Reference element
20 8.4.5 Long-term stability
8.4.6 Preliminary instrument check
8.5 Calibration
8.5.1 Linear calibration function
21 8.5.2 Standard addition calibration
8.6 Solutions to be prepared
8.6.1 General
8.6.2 Blank calibration solution
8.6.3 Blank test solution
8.6.4 Calibration solutions
22 8.6.5 Test sample solutions
8.6.6 Test solutions
8.7 Measurement procedure
23 11.1 Calibration check
11.2 Interference
24 11.3 Recovery
11.4 Performance data

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BS EN ISO 22036:2024
$167.15