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BS EN IEC 62554:2011+A1:2018

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Sample preparation for measurement of mercury level in fluorescent lamps

Published By Publication Date Number of Pages
BSI 2018 28
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This International Standard specifies sample preparation methods for determining mercury levels in new tubular fluorescent lamps (including single capped, double capped, self-ballasted and CCFL for backlighting) containing 0,1 mg mercury or more. The intended resolution of the methods described in this standard is of the order of 5 %.

Mercury level measurement of spent lamps is excluded, as during lamp operation, mercury gradually diffuses into the glass wall and reacts with the glass materials. The test method of this standard does not recover mercury that is diffused into or reacted with or otherwise incorporated irreversibly with the glass wall of discharge tubes.

This standard does not contain information on measurement. Measurement is specified in IEC 62321.

PDF Catalog

PDF Pages PDF Title
2 National foreword
4 European Foreword
5 European foreword to amendment A1
6 Annex ZA (normative) Normative references to international publications with their corresponding European publications
8 FOREWORD
10 INTRODUCTION
11 1 Scope
2 Normative references
3 Terms and definitions
4 General
12 5 Procedure for collecting mercury from a fluorescent lamp
5.1 General
5.2 Reagents
5.3 Chemical lab ware
13 5.4 Sample preparation
5.4.1 Cold spotting methods
15 5.4.2 Sample preparation of fluorescent lamps by non-cold-spot (sectioning) methods
16 5.4.3 Sample preparation of fluorescent lamps by non-cold-spot (crushing) methods
17 5.4.4 Nitric acid rinse method for linear fluorescent lamps
18 5.4.5 Direct mercury measurement
5.4.6 Sample preparation of other fluorescent lamps
5.5 Sample digestion
5.5.1 Ambient conditions
5.5.2 Glass samples (in 250 ml, 500 ml, 1 000 ml or 2 000 ml container)
19 5.6 Filtering
6 Measurement
6.1 Blank test
6.2 Data reporting
6.3 Analysis
20 Annex A (informative) Electrothermal vaporization atomic absorption spectrometry (EVAAS) method
23 Annex B (informative) Information on the cold spotting method
27 Bibliography
BS EN IEC 62554:2011+A1:2018
$142.49