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BS 6057-3.13:1993:2006 Edition

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Rubber latices. Methods of test – Determination of sludge content

Published By Publication Date Number of Pages
BSI 2006 8
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Method is not applicable to compounded latex or vulcanized latex.

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1 BRITISH STANDARD
BS 6057-3.13: 1993
ISO 2005:1992
Rubber latices –
Part 3: Methods of test –
Section 3.13 Determination of sludge content
NOTE Attention is drawn to BS 6057-0 “General introduction”, issued separately
2 This British Standard, having been prepared under the direction of the Plastics and Rubber Standards Policy Committee, was published under the authority of the Standards Board and comes into effect on 15 January 1993
© BSI 2006
First published January 1984
Second edition December 1987
The following BSI references relate to the work on this standard:
Committee reference PRM/51
Committees responsible for this British Standard
3 Contents
4 National foreword
5 1 Scope
2 Normative reference
3 Principle
4 Reagents
4.1 Ammonia and alcohol, solution having the following composition:
5 Apparatus
5.1 Centrifuge, producing a mean acceleration of approximately 12 000 m/s2, with two 50 cm3 conical centrifuge tubes.
5.2 Pipette, of suitable capacity, having a tip opening of diameter approximately 2 mm.
6 Sampling
7 Procedure
8 Expression of results
9 Precision statement
9.1 The precision of this method was determined in accordance with ISO/TR 9272. Refer to this document for terminology and explanations of statistical concepts.
9.2 The precision details in this precision statement give an estimate of the precision of this test method with the materials u…
6 9.3 The precision results are given in Table 1. The precision is expressed on the basis of a 95 % confidence level for the values established for repeatability r and reproducibility R.
9.4 The results contained in Table 1 are mean values and give an estimate of the precision of this test method as determined in …
9.5 A type 1 precision was determined, based on the sampling method used for the latex samples in the ITP.
9.6 Repeatability: The repeatability r (in measurement units) of this test method has been established as the appropriate value …
9.7 Reproducibility: The reproducibility R (in measurement units) of this test method has been established as the appropriate va…
9.8 Bias: In test method terminology, bias is the difference between an average test value and the reference (or true) test property value.
Table 1 – Estimate of precision of determination of sludge content
r = 2,83 × sr
where r is the repeatability (in measurement units) and sr is the within-laboratory standard deviation.
R = 2,83 × sR
where R is the reproducibility (in measurement units) and sR is the between-laboratory standard deviation.
10 ” Test report
a) a reference to this International Standard;
b) all details necessary for identification of the test sample;
c) the results, and the units in which they have been expressed;
d) any unusual features noted during the determination;
e) any operation not included in this International Standard or in the International Standard to which reference is made, as well as any operation regarded as optional.
7 List of references
8 BS 6057-3.13: 1993 ISO 2005:1992
BS 6057-3.13:1993
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